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In a clean result you want one dominant peak (or multiple dominant peaks for blends), which shows the sample is almost entirely the intended peptide

This is generally related to the caloric deficit rather than the medication itself, and it typically resolves as caloric intake stabilizes

Physiol Res

However, the detection window depends heavily on which metabolites are targeted

The 500 mcg per-capsule dose mirrors the per-day intake used in the bulk of rodent oral studies, and the gastric origin of the parent molecule provides a biological rationale for stability through the GI tract a feature documented across multiple oral-administration preclinical models