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An Atlantis Premier BEH Z-HILIC FIT Column (2.1 mm 100 mm, 1.7 m), equipped with an integrated guard column (Vanguard FIT), was used for the separation, with aqueous mobile phase consisting of 10 mM ammonium acetate (pH 9.1, adjusted with NH 4 OH) in double-deionized water and organic mobile phase consisting of 0.1% formic acid in acetonitrile

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