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Compound 4 (1.94 g, 2.47 mmol), H-Lys-OMe2HCl (0.24 g, 1.03 mmol), PYBOP (1.62 g, 3.10 mmol) and HOBT (0.42 g, 3.10 mmol) were dissolved in DMF (40 mL) under nitrogen atmosphere and ice bath conditions

IR-/ER-Tac (roughly 17%), while Cmin only differed slightly to ER- (6% lower) and IR-Tac (3% higher)